Көмірсутек материалдарының ИҚ Фурье-спектроскопиясы үшін төмен температуралық ұяшықты әзірлеу.
DOI:
https://doi.org/10.31489/2025N2/88-96Кілт сөздер:
FTIR спектроскопиясы, төмен температура, ұяшық, криогенді капиллярлық жүйе, көмірсутекті материалдарАңдатпа
Бұл жұмыста көмірсутекті материалдардың төмен температурада және атмосфералық қысымда FTIR спектроскопия технологиясы көрсетілген. Бұл құрылғы әртүрлі заттардың оптикалық қасиеттерін 77 – 300 К температура диапазонында вакуумсыз зерттеуге және бұл салада зерттеулер жеткіліксіз болғандықтан жаңа іргелі мәліметтер алуға мүмкіндік береді. Сипатталған жаңа әдістер мен әдістемелер FTIR спектрометрімен, диффузиялық шағылыстыру қондырғысымен және екі Дьюар ыдысымен жұмыс істейді, криогендік капиллярлық жүйеде сұйық азотпен салқындату және ИҚ-белсенді емес ортаны құру үшін газды азотпен үрлеу. Бұл жаңа әдістемені теориялық ақпарат ретінде білім беру саласымен қатар әртүрлі энергетикалық және инфрақұрылымдық салалар үшін пайдалы принципті жаңа деректерді алудың құнды әдісіне айналдырады.
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