Разработка низкотемпературной ячейки для ИК Фурье-спектроскопии углеводородных материалов.
DOI:
https://doi.org/10.31489/2025N2/88-96Ключевые слова:
ИК Фурье-спектроскопия, низкая температура, ячейка, криогенная капиллярная система, углеводородные материалыАннотация
В данной работе представлена технология ИК-Фурье спектроскопии углеводородных материалов при низких температурах и атмосферном давлении. Это устройство позволяет изучать оптические свойства различных веществ в диапазоне температур 77 – 300 К без необходимости использования вакуума и получать новые фундаментальные данные, поскольку исследований в этой области недостаточно. Описаны новые методики и методы работы с ИК-Фурье спектрометром, приставкой диффузного отражения и двумя сосудами Дьюара, использующими для охлаждения жидким азотом внутри криогенной капиллярной системы и продувки газообразным азотом для создания ИК-неактивной среды. Это делает новую методику ценным методом получения принципиально новых данных, полезных для различных сфер энергетики и инфраструктуры, а также для области образования в качестве теоретической информации.
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